The comparative analysis of the solid-state 31P NMR spectra of Re-Pt vinylidene complexes

Описание

Тип публикации: доклад, тезисы доклада, статья из сборника материалов конференций

Конференция: International Scientific Conference on Applied Physics, Information Technologies and Engineering 2019, APITECH 2019

Год издания: 2019

Идентификатор DOI: 10.1088/1742-6596/1399/2/022028

Аннотация: The two vinylidene complexes Cp(CO)2 RePt(μ-C=CHPh)(PPh3 )(CO) and Cp(CO)2 RePt(μ-C=CHPh)(PPh3 )2 and their precursors PPh3 and P(PPh3 )4 were studied by solid-state nuclear magnetic resonance. We analysed 31P cross-polarization spectra acquired in static conditions and with magic angle spinning. The chemical shift tensors of each Показать полностьюsample were determined by fitting their spectra using SIMPSON simulations. © Published under licence by IOP Publishing Ltd.

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Издание

Журнал: Journal of Physics: Conference Series

Выпуск журнала: Vol. 1399, Is. 2

Номера страниц: 22028

ISSN журнала: 17426588

Издатель: Institute of Physics Publishing

Авторы

  • Smolyarov K.T. (Federal Research Center, Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences (KSC SB RAS), Krasnoyarsk, Russian Federation, Siberian Federal University, Krasnoyarsk, Russian Federation)
  • Volkov N.V. (Siberian Federal University, Krasnoyarsk, Russian Federation)
  • Matsulev A.N. (Kirensky Institute of Physics SB RAS, Krasnoyarsk, Russian Federation, Institute of Chemistry and Chemical Technology SB RAS, Krasnoyarsk, Russian Federation)
  • Kondrasenko A.A. (Kirensky Institute of Physics SB RAS, Krasnoyarsk, Russian Federation, Institute of Chemistry and Chemical Technology SB RAS, Krasnoyarsk, Russian Federation)

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