Hydroxyethyl Urea Crystal Hydrate: Experimental and Theoretical Study

Описание

Тип публикации: статья из журнала

Год издания: 2026

Идентификатор DOI: 10.1142/S273741652550084X

Ключевые слова: Hydroxyethylurea, crystalline hydrate, dft, QTAIM, elf, LoL

Аннотация: <jats:p> Hydroxyethyl urea (HEU) is an important urea derivative that finds wide application in various fields from cosmetics to a component of low-freezing batteries. In all areas of its application, special attention is paid to noncovalent interactions with water. In this work, we investigated the noncovalent interactions of HEU Показать полностьюwith water and also obtained and studied the crystal hydrate of this substance. The obtained crystal hydrates were studied by experimental and theoretical methods. Thus, the incorporation of water molecules into the HEU crystal leads to a broadening of the characteristic peaks in FTIR, and on diffractograms, it affects the change of peak intensity. The calculation results indicate that the hydrogen (H) atoms bonded to the nitrogen atoms of HEU represent the nucleophilic region. The area around the oxygen (O) atoms of HEU represents the electrophilic region. The O–H[Formula: see text]O hydrogen bond lengths in HEU-n ⋅ W ([Formula: see text] 1–12) clusters range from 1.685 Å to 2.066 Å, with electron densities between 0.0178 and 0.0456 au and bond energies of 3.891–13.491 kcal/mol. N–H[Formula: see text]O hydrogen bonds exhibit lengths of 1.900–2.116 Å, electron densities of 0.0185–0.0287 au, and bond energies between 3.671 kcal/mol and 6.808 kcal/mol. Reduced Density Gradient (RDG) analysis confirmed that hydrogen bonding is the dominant interaction in the formation of HEU hydrates. </jats:p>

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Издание

Журнал: Journal of Computational Biophysics and Chemistry

Выпуск журнала: Т. 25, 9

Номера страниц: 1285-1300

ISSN журнала: 27374165

Издатель: World Scientific

Персоны

  • Holikulov Utkirjon (Samarkand State University)
  • Kazachenko Aleksandr S. (Prof. V.F. Voino-Yasenetsky Krasnoyarsk State Medical University of the Ministry of Healthcare of the Russian Federation)
  • Issaoui Noureddine (University Monastir)
  • Al-Dossary Omar M. (King Saud University)
  • Ponomarev Ilya S. (Krasnoyarsk Science Center, Siberian Branch, Russian Academy of Sciences)
  • Kazachenko Anna S. (Siberian Federal University)
  • Malyar Yuriy N. (Krasnoyarsk Science Center, Siberian Branch, Russian Academy of Sciences)
  • Bousiakou Leda G. (IMD Laboratories Co, R&amp;D Section, Lefkippos Technology Park, NCSR Demokritos)

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